Study on the effects of Zr content on the PbO-ZrO₂-TiO₂ system at 1100°C

Authors

Romena de Chavez ⋅ PH Institute of Mathematical Sciences and Physics, University of the Philippines Los Baños
Marvin U. Herrera ⋅ PH Institute of Mathematical Sciences and Physics, University of the Philippines Los Baños
Josefina Celorico ⋅ PH Industrial Technology Development Institute, Department of Science and Technology

Abstract

This paper investigates the effect of varying amount of Zr on the physical properties of PbO-ZrO₂-TiO₂ system at 1100°C . Samples were characterized using different characterization techniques such as Differential Thermal Analysis (DTA), X-ray diffraction (XRD), Scanning Electron Microscopy (SEM), and porosity test. XRD data shows that increasing amount of Zr caused increase in formation of PTO rather than PZT. Among the composition studied, the sample with 0.2 mole fraction of Zr has the lowest melting point, highest porosity and lowest bulk density. At the said composition, XRD shows the occurrence of both PTO and PZT in large amount. Also, SEM images show the occurrence of stripy microstructure that could signify the inhomogeneous mixture of the two compounds.

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Issue

2006: Proceedings of the 24th Samahang Pisika ng Pilipinas National Physics Congress

Article ID

SPP-2006-1F-02

Section

Materials Science

Published

2006-10-25

How to Cite

[1]

R de Chavez, MU Herrera, and J Celorico, Study on the effects of Zr content on the PbO-ZrO2-TiO2 system at 1100°C , Proceedings of the Samahang Pisika ng Pilipinas 24, SPP-2006-1F-02 (2006). URL: https://proceedings.spp-online.org/article/view/SPP-2006-1F-02.