Synthesis of Bi-2212 via coprecipitation using oxalic acid and triethylamine solution

Authors

Jonee Christine P. Zuñega ⋅ PH Materials Science and Engineering Program, University of the Philippines Diliman
J. R. Layug ⋅ PH Materials Science and Engineering Program, University of the Philippines Diliman
Roland V. Sarmago ⋅ PH National Institute of Physics, University of the Philippines Diliman

Abstract

Bi-2212 was successfully synthesized from a coprecipitation process using oxalate and triethylamine solution as precipitants. Basic chemical reactions were used to calculate for the corresponding amounts of precursors and precipitants at varying amounts of oxalate. Characterization was carried out using XRD, SEM and magnetic susceptibility measurements. XRD after sintering showed that the peaks observed belong to Bi-2212 phase with varying T_c's of 83K, 64K and 70K. SEM showed enhanced formation of platelike grains with less porosity.

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Issue

2002: Proceedings of the 20th Samahang Pisika ng Pilipinas Physics Congress

Article ID

SPP-2002-2D-04

Section

Condensed Matter and Plasma Physics

Published

2002-10-23

How to Cite

[1]

JCP Zuñega, JR Layug, and RV Sarmago, Synthesis of Bi-2212 via coprecipitation using oxalic acid and triethylamine solution, Proceedings of the Samahang Pisika ng Pilipinas 20, SPP-2002-2D-04 (2002). URL: https://proceedings.spp-online.org/article/view/SPP-2002-2D-04.